تفاعل #54526
ord-89c4a44e39b04448b933484d36cfabda
معادلة التفاعل
cyclohexene oxide
dimethylamine
hydrochloride
→
trans-2-Dimethylaminocyclohexanol
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرى67, 63899 d, Rocz
الإجراء التجريبي
This compound was previously prepared from cyclohexene oxide and dimethylamine in benzene at room temperature for 14 days in 95% yield, b.p. 90° (20 mm): J. Chem. Soc., 4835 (1965); or in autoclave: C. A. 67, 63899 d, Rocz. Chem. 41, 541 (1967) b.p. 88° (14 mm); also Bull. Soc. Chim. France, 850 (1947): hydrochloride and resolution reported.