تفاعل #53760

ord-868776c4aa2e4da9aec0e9e64cce3e8d

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The process is performed as in Example 1 with, in the first reactor, 168 g (4 mol) of sodium fluoride powder having the same characteristics as described in Example 1 and 320 ml of acetonitrile and, in the second reactor, 108 g (1 mol) of benzyl alcohol, 50.5 g (1.2 mol) of sodium fluoride of the same characteristics as above and 150 g of dimethoxyethane.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US06858751B1uspto-grants-2005_02