تفاعل #53313

معادلة التفاعل

Triethylamine

Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromobutyrate

→

title compound

Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-3-butenoate

المذيبات

carbon tetrachloride

ظروف التفاعل

المعالجة

1. 1
   ترشيحthe mixture can be filtered through a pad of silica gel few times
2. 2
   تركيزconcentrate

الإجراء التجريبي

Add Triethylamine to a solution of Ethyl 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-bromobutyrate (Step E) in carbon tetrachloride. After stirring approximately for 4 hours, the mixture can be filtered through a pad of silica gel few times, and concentrate to give the title compound.

المصدر