تفاعل #532787

ord-afeab43bba1444e7aaaf40b879ad7a5f

معادلة التفاعل

Oc1cncc(Br)c1
3-bromo-5-hydroxypyridine
CC(C)O
isopropanol
CC(C)Oc1cncc(Br)c1
title compound
CC(C)Oc1cncc(Br)c1
3-Bromo-5-isopropoxypyridine

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThe title compound was synthesized in a similar manner

الإجراء التجريبي

The title compound was synthesized in a similar manner as described for Stage 29.1.1 using 3-bromo-5-hydroxypyridine (Aldrich, Buchs, Switzerland) and isopropanol (Merck, Dietikon, Switzerland) to give the title compound as a colorless oil. (HPLC: tR 2.92 min (Method A); M+H=216, 218 MS-ES).

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US08476294B2uspto-grants-2013_07