تفاعل #531840

معادلة التفاعل

2-allyl-5-methylthiophene

trichlorosilane

→

2-(3-Trichlorosilylpropyl)-5-methylthiophene

المذيبات

toluene

ظروف التفاعل

المعالجة

1. 1
   أخرىThe hydrosilylation reaction of Example 1

الإجراء التجريبي

The hydrosilylation reaction of Example 1 was repeated using 4.5 g of 2-allyl-5-methylthiophene in place of 2-allylthiophene, 2.5 g of anhydrous toluene, 5.0 g of trichlorosilane, and 50 mg of Platinum Catalyst. 2-(3-Trichlorosilylpropyl)-5-methylthiophene was obtained as a colorless liquid: 1H NMR (CDCl3) δ 6.60 (m, 2H); 2.88 (t, 2H, J=7.2 Hz); 2.47 (s, 3H); 1.95 (m, 2H); 1.47 (m, 2H).

المصدر