تفاعل #531791

معادلة التفاعل

Mercaptopropionic acid

Triphenylmethylchloride

→

3-(tritylthio)propionic acid

المردود 95.7%

المذيبات

methylene chloride

ظروف التفاعل

المعالجة

1. 1
   أخرىwere carried out at room temperature
2. 2
   ترشيحwas gathered by filtration
3. 3
   أخرىthe solid components obtained here
4. 4
   أخرىwere dried under reduced pressure

الإجراء التجريبي

Mercaptopropionic acid 12 (3.14 g) was dissolved in 50 ml of methylene chloride. Triphenylmethylchloride 13 (8.36 g) was added to that, and 19-hour reactions were carried out at room temperature. The precipitate generated through the reactions was gathered by filtration, and the solid components obtained here were dried under reduced pressure, to form 9.86 g of 3-(tritylthio)propionic acid 14, which is a white solid.

المصدر