تفاعل #53104

ord-d8fcf8522f2743eb9fc11796f1587bf2

معادلة التفاعل

CCOC(=C1C(=O)Nc2ccc([N+](=O)[O-])cc21)c1ccccc1
3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone
CCOC(=O)CNCc1cccc(N)c1
3-ethoxycarbonylmethylaminomethyl-aniline
→
CCOC(=O)CNCc1cccc(N/C(=C2\C(=O)Nc3ccc([N+](=O)[O-])cc32)c2ccccc2)c1
(Z)-3-[1-(3-ethoxycarbonylmethylaminomethyl-phenylamino)-1-phenyl-methylidene]-5-nitro-2-indolinone

المتفاعلات

CCOC(=C1C(=O)Nc2ccc([N+](=O)[O-])cc21)c1ccccc1
3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone
CCOC(=O)CNCc1cccc(N)c1
3-ethoxycarbonylmethylaminomethyl-aniline

الكواشف

لا شيء

المذيبات

CN(C)C=O
DMF

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

Prepared analogously to Example 89 from 3-(1-ethoxy-1-phenyl-methylidene)-5-nitro-2-indolinone and 3-ethoxycarbonylmethylaminomethyl-aniline in DMF.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US06855710B2uspto-grants-2005_02