تفاعل #527364

ord-81f4e5c0251d4fa980836e89a829f84c

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

Chlorotrifluoroethylene of the formula (7) is treated with n-butyl lithium and then reacted with chlorotrimethylsilane of the formula (8) to obtain 1,1,2-trifluoro-2-trimethylsilylethylene of the formula (9). Then, without isolation, this compound (9) is reacted further with a lithium compound of the formula (10) to obtain a difluoroethylene compound of the formula (11).

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05516949uspto-grants-1996_05