تفاعل #52585

معادلة التفاعل

5-Fluoroisatin

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title compound

5-Fluoro-2-oxindole

المذيبات

hydrazine hydrate

—

ice water

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةrefluxed for 1.0 hr
2. 2
   أخرىThe reaction mixtures
3. 3
   ترشيحThe precipitate was then filtered
4. 4
   غسيلwashed with water
5. 5
   أخرىdried in a vacuum oven

الإجراء التجريبي

5-Fluoroisatin (8.2 g) was dissolved in 50 mL of hydrazine hydrate and refluxed for 1.0 hr. The reaction mixtures were then poured in ice water. The precipitate was then filtered, washed with water and dried in a vacuum oven to afford the title compound.

المصدر