تفاعل #51741
ord-5b61d909b51a46b58d8de41f946ae5e3
معادلة التفاعل
2-(methyloxycarbonyl)amino-4-isopropyl-7-methyl-6-thiocyanato-benzothiazole
dithiothreitol
phosphate
→
title compound
2-(Methyloxycarbonyl)amino-4-isopropyl-7-methyl-benzothiazole-6-thiol
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
The title compound was prepared according to General Method 14 using 2-(methyloxycarbonyl)amino-4-isopropyl-7-methyl-6-thiocyanato-benzothiazole (1.5 g, 4.7 mmol), dithiothreitol (2.9 g, 18.7 mmol), EtOH (50 mL), and phosphate buffer (15 mL). MS (APCI): 296 (M−H).