تفاعل #51738
ord-10295e2b277a470283758c831ee5ebe7
معادلة التفاعل
7-isopropyl-4-methyl-6-thiocyanato-benzothiazol-2-yl-amine
dithiothreitol
phosphate
→
title compound
2-Amino-7-isopropyl-4-methyl-benzothiazole-6-thiol
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
The title compound was prepared according to General Method 14 using 7-isopropyl-4-methyl-6-thiocyanato-benzothiazol-2-yl-amine (Example L-5; 11.5 g, 43.7 mmol), dithiothreitol (27.0 g, 175 mmol), EtOH (200 mL), and phosphate buffer (50 mL). MS (APCI): 239 (M+H).