تفاعل #51737
ord-cbb2200b505743f89d88f8471e6e0c7a
معادلة التفاعل
5-tert-butyl-6-thiocyanato-benzothiazol-2-yl-amine
dithiothreitol
phosphate
→
title compound
2-Amino-5-tert-butyl-benzothiazole-6-thiol
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
The title compound was prepared according to General Method 14 using 5-tert-butyl-6-thiocyanato-benzothiazol-2-yl-amine (Example L-1; 8 g, 30 mmol), dithiothreitol (18.7 g, 121 mmol), EtOH (200 mL), and phosphate buffer (50 mL). MS (APCI): 239 (M+H).