تفاعل #51463

معادلة التفاعل

N-Boc sarcosine piperonylamide

acetyl chloride

→

sarcosine piperonyl amide hydrochloride

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   أخرىall volatiles were removed under reduced pressure

الإجراء التجريبي

N-Boc sarcosine piperonylamide (500 mg, 1.54 mmol) in methanol (10 mL) was treated with acetyl chloride (1 mL). After 45 minutes, all volatiles were removed under reduced pressure to yield sarcosine piperonyl amide hydrochloride (395 mg, quant.) as a sticky solid.

المصدر