تفاعل #51376

معادلة التفاعل

N-Phenylacetyl-L-leucine

iso-butyl alcohol

→

N-(phenylacetyl)-L-leucine iso-butyl ester

المذيبات

CHCl3

ظروف التفاعل

المعالجة

1. 1
   ترشيحfiltered through a plug of cotton
2. 2
   أخرىthe filtrate evaporated at reduced pressure to an oil which

الإجراء التجريبي

N-Phenylacetyl-L-leucine (0.0081 g, 0.038 mmol) was dissolved in 2.0 mL CHCl3 (EtOH free) and iso-butyl alcohol (0.055 mL) and treated with P-EPC (100 mg, 0.87 milliequivalents). The mixture was rotated for 4 days, filtered through a plug of cotton and the filtrate evaporated at reduced pressure to an oil which was sufficiently pure for testing.

المصدر