تفاعل #51327

ord-d5613df61c1a406e8d4bc734c58fdd6b

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThe reaction was monitored by tlc on silica gel (Rf=0.9 in 3% methanol/methylene chloride) and purification

الإجراء التجريبي

Following General Procedure AH above and using N-(3,5-difluorophenyl)alanine (from Example AC above) and iso-butanol, the title compound was prepared as an oil. The reaction was monitored by tlc on silica gel (Rf=0.9 in 3% methanol/methylene chloride) and purification was by preparative plate chromatography (silica gel using 3% methanol/methylene chloride as the eluant).

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US06849650B2uspto-grants-2005_02