تفاعل #50708

معادلة التفاعل

8-phenyloctyl chloride

sodium iodide

→

8-phenyloctyl iodide

المذيبات

acetone

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةwas heated
2. 2
   درجة الحرارةunder reflux for 20 hours
3. 3
   أخرىEvaporated
4. 4
   workup.ADDITIONwater (20 ml) added
5. 5
   استخلاصextracted with diethyl ether (20 ml)
6. 6
   أخرىThe extracts were dried
7. 7
   ترشيحfiltered
8. 8
   أخرىevaporated to a pale yellow liquid (5.5 g)
9. 9
   workup.DISTILLATIONDistilled

الإجراء التجريبي

A mixture of 8-phenyloctyl chloride (4.4 g), sodium iodide (5.34 g) and acetone (20 ml) was heated under reflux for 20 hours. Evaporated, water (20 ml) added and extracted with diethyl ether (20 ml). The extracts were dried, filtered and evaporated to a pale yellow liquid (5.5 g). Distilled to give 8-phenyloctyl iodide, b.p. 200° C. (air bath temperature) at 0.1 mBar.

المصدر