تفاعل #49904

معادلة التفاعل

N'-t-butyl-N-(thiobenzoyl)hydrazine

m-toluoyl chloride

toluene

→

N'-t-butyl-N-(thiobenzoyl)-N'-(3-toluoyl)hydrazine

المذيبات

water

ظروف التفاعل

المعالجة

1. 1
   أخرىat 23° C
2. 2
   أخرىthe product was isolated by filtration (0.25 g)

الإجراء التجريبي

N'-t-butyl-N-(thiobenzoyl)hydrazine (ca. 1 g), m-toluoyl chloride (approx. 0.7 g) and 50% aqueous sodium hydroxide (6 drops) were mixed in 1 ml water and 10 ml toluene at 23° C. After stirring for 3 hours, ether-hexane was added and the product was isolated by filtration (0.25 g): m.p. 165°-168° C.

المصدر