تفاعل #49902

معادلة التفاعل

1,1-dimethylethylhydrazine oxalate

benzoyl chloride

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product

المردود 15.0%

N'-(1,1-dimethylethyl)-N,N'-dibenzoylhydrazine

المردود 15.0%

المذيبات

toluene

sodium hydroxide

sodium hydroxide

hexane

ظروف التفاعل

المعالجة

1. 1
   ترشيحfiltered

الإجراء التجريبي

The 1,1-dimethylethylhydrazine oxalate (2 g) was dissolved in toluene and neutralized with 50% aqueous sodium hydroxide. To this solution was added benzoyl chloride (4.02 g) and sodium hydroxide (50% Aq. solution) (2.45 g) at 25° C. The reaction mixture was warmed to room temperature and stirred 3 hours. The mixture was diluted with hexane and filtered to afford the product as a white solid (0.5 g).

المصدر