تفاعل #49704

ord-2394b2dec9d049a3b2e5b53f9d321778

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

To a solution of 4-hydroxy-4'-octylbiphenyl (0.5 g) and terephthaloyl chloride (0.36 g) in about dichloromethane (30 ml) was added drop by drop triethylamine (0.2 g). To the solution was added dimethylaminopyridine (0.013 g) and the mixture was stirred at the room temperature for 10 hours to obtain the titled compound.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05424005uspto-grants-1995_06