تفاعل #48898

معادلة التفاعل

1,2,3-propanetricarboxylic acid

2-methylcyclohexylamine

→

1,2,3-propanetricarboxylic acid tris(2-methylcyclohexylamide)

المذيبات

xylene

ظروف التفاعل

المعالجة

1. 1
   أخرىobtained above, and the contents
2. 2
   درجة الحرارةwere refluxed
3. 3
   درجة الحرارةunder heating
4. 4
   أخرىreacted for 3 hours

الإجراء التجريبي

Next, 3.52 g (20 mmol) of 1,2,3-propanetricarboxylic acid (made by Nacalai Tesque) and 13.6 g (120 mmol) of 2-methylcyclohexylamine were added to the xylene solution of a tricresol boric acid ester obtained above, and the contents were refluxed under heating and reacted for 3 hours. This gave a crude 1,2,3-propanetricarboxylic acid tris(2-methylcyclohexylamide) as a white solid.

المصدر