تفاعل #487529

ord-74aa5e5576d7455fa7be6743a8818c9c

معادلة التفاعل

CCCCCC.CCOC(C)=O
Ethyl acetate Hexane
CCCCCCCC/C=C\CCCCCCCC(=O)Cl
Oleoyl chloride
C=CCCCCCCCCO
9-decen-1-ol
→
C=CCCCCCCCCOC(=O)CCCCCCC/C=C\CCCCCCCC
Compound F
المردود 97.5%
C=CCCCCCCCCOC(=O)CCCCCCC/C=C\CCCCCCCC
Dec-9-enyl oleate
المردود 97.5%

المتفاعلات

CCCCCC.CCOC(C)=O
Ethyl acetate Hexane
CCCCCCCC/C=C\CCCCCCCC(=O)Cl
Oleoyl chloride
C=CCCCCCCCCO
9-decen-1-ol
—
compound F

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

Compound F was prepared from Oleoyl chloride and 9-decen-1-ol following the general procedure already discussed and shown in FIG. 11. Pure compound F was a colorless oil obtained by column chromatography with Ethyl acetate/Hexane=1:40.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US08741822B2uspto-grants-2014_06