تفاعل #484403

معادلة التفاعل

diallylmethylamine

1,10-dibromodecane

→

product

1,10-Bis(diallylmethylammonio)decane Dibromide

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةto cool to room temperature
2. 2
   أخرىThe solvent was removed by rotary vacuum evaporation
3. 3
   workup.ADDITIONDiethylether (400 mL) was added
4. 4
   أخرىthe top layer was decanted
5. 5
   أخرىThe remaining oil was dried by rotary vacuum evaporation

الإجراء التجريبي

To a 1 L Morton flask was added diallylmethylamine (86.1 g), 1,10-dibromodecane (112 g), and methanol (100 mL). The mixture was heated to 65° C. for 24 h, and then allowed to cool to room temperature. The solvent was removed by rotary vacuum evaporation. Diethylether (400 mL) was added and the mixture was stirred for 1 hr. The mixture was allowed to settle and the top layer was decanted and discarded. The remaining oil was dried by rotary vacuum evaporation to yield 215 g of product.

المصدر