تفاعل #481596
ord-83c72e353ec04bd482eb10dab9a2277c
معادلة التفاعل
zirconium hydroxide
nitric acid
cerium
lanthanum
zirconium hydroxide
zirconium oxychloride
→
zirconium oxide
cerium oxide
lanthanum oxide
المتفاعلات
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1workup.ADDITIONmixing them together
- 2workup.ADDITIONby addition of an alkali,
- 3غسيلwashing
- 4أخرىdrying at 120° C. for two hours
الإجراء التجريبي
A zirconium-cerium-lanthanum composite oxide (Powder A1) was obtained by hydrolyzing a zirconium oxychloride solution thereby obtaining zirconium hydroxide, adding an aqueous nitric acid solution of cerium and lanthanum to the zirconium hydroxide and mixing them together, neutralizing the resultant mixture by addition of an alkali, washing, drying at 120° C. for two hours and calcining at 700° C. for one hour the product of neutralization, with the relevant components used in amounts calculated to form a weight ratio of 40 g of zirconium oxide, 20 g of cerium oxide, and 15 g of lanthanum oxide.