تفاعل #4712

معادلة التفاعل

methylisothiocyanate

N-[3-[3-(1-piperidinylmethyl) phenoxy]propyl]-hydrazine carboxamide

→

2-(Methylaminothioxomethyl)-N-[3-[3-(1-piperidinylmethyl)phenoxy]-propyl]-hydrazine carboxamide

المذيبات

THF

ظروف التفاعل

المعالجة

1. 1
   أخرىThe precipitate obtained
2. 2
   ترشيحis filtered off
3. 3
   أخرىrecrystallised from ethanol

الإجراء التجريبي

0.5 g (6.6 mmol) of methylisothiocyanate are added to 1.0 g (3.3 mmol) of N-[3-[3-(1-piperidinylmethyl) phenoxy]propyl]-hydrazine carboxamide in 20 ml of THF and the mixture is stirred at room temperature for 12 hours. The precipitate obtained is filtered off and recrystallised from ethanol. The analytical values are summarized in Table I.

المصدر