تفاعل #470370

معادلة التفاعل

sodium trifluoroacetate

N-methoxymethyl-N-methylpyrrolidinium chloride

N-Methyl-N-Methoxymethylpyrrolidinium Chloride

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colorless liquid

N-Methoxymethyl-N-Methylpyrrolidinium trifluoroacetate

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   تركيزconcentrated in a vacuum
2. 2
   أخرىdried in a vacuum
3. 3
   workup.DISSOLUTIONThe residue was dissolved in 500 ml of dichloromethane
4. 4
   ترشيحfollowed by filtration with a membrane
5. 5
   ترشيحfilter
6. 6
   تركيزconcentration in a vacuum
7. 7
   أخرىdrying

الإجراء التجريبي

A 14.94 g quantity of sodium trifluoroacetate was dissolved in 100 g of methanol, and 18.20 g of N-methoxymethyl-N-methylpyrrolidinium chloride was added to the solution at room temperature. The mixture was stirred for 1 hour, concentrated in a vacuum and dried in a vacuum using a vacuum pump. The residue was dissolved in 500 ml of dichloromethane, followed by filtration with a membrane filter, concentration in a vacuum and drying, affording 26.52 g of a colorless liquid as the desired product.

المصدر