تفاعل #470367

معادلة التفاعل

Methoxymethylpyrrolidine

dimethyl carbonate

→

desired product

المردود 60.0%

N-Methoxymethyl-N-Methylpyrrolidinium Methyl carbonate

المردود 60.0%

ظروف التفاعل

المعالجة

1. 1
   أخرىreacted at 120° C. for 24 hours
2. 2
   ترشيحThe resulting solids were filtered off
3. 3
   غسيلwashed with dimethyl carbonate
4. 4
   أخرىThe solids were dried in a vacuum

الإجراء التجريبي

Methoxymethylpyrrolidine (10.00 g) and 117.39 g of dimethyl carbonate were placed into an autoclave and reacted at 120° C. for 24 hours. The resulting solids were filtered off and washed with dimethyl carbonate. The solids were dried in a vacuum, giving 10.70 g of the desired product.

المصدر