تفاعل #465953
ord-c4b88dc8fc2f43d4a6be06585468b591
معادلة التفاعل
hexyl t-butyl ether
t-butanol
1-hexanol
N2
hexanol
→
t-Butyl Ether
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
300 mmoles of t-butanol, 100 mmoles of 1-hexanol and 2.5 g of Ti-Si-catalyst powder are stirred in a 100 ml autoclave at a pressure of 40 bar N2 and a temperature of 150° C. over a period of 17 h, 17% of n hexanol were converted into hexyl t-butyl ether with a selectivity of 90%.