تفاعل #465952
ord-6a5710d67e814d708dc3e64c5f91b38a
معادلة التفاعل
hexyl-t-butyl ether
i-butene
1-hexanol
N2
n-hexanol
→
t-Butyl Ether
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
300 mmoles of i-butene, 100 mmoles of 1-hexanol and 2.5 g of Ti-Si-catalyst powder are stirred in a 100 ml autoclave at a pressure of 40 bar N2 and a temperature of 150° C. over a period of 18 h, 62% of n-hexanol were converted into hexyl-t-butyl ether with a selectivity of 92%.