تفاعل #458447

معادلة التفاعل

1,10-dibromodecane

sodium benzyloxide

→

10-Benzyloxydecanyl bromide

المذيبات

tetrahydrofuran

ظروف التفاعل

المعالجة

1. 1
   ترشيحfiltering the precipitated material
2. 2
   تركيزconcentrating the filtrate
3. 3
   workup.DISTILLATIONdistilling the concentrated filtrate under reduced pressure

الإجراء التجريبي

10-Benzyloxydecanyl bromide was prepared by reacting 100 g of 1,10-dibromodecane with an equimolar amount of sodium benzyloxide in tetrahydrofuran under reflux conditions, filtering the precipitated material, concentrating the filtrate and distilling the concentrated filtrate under reduced pressure. Yield 46 g. B.P. 185° to 189° C./3 mmHg.

المصدر