تفاعل #452418
ord-f0c77084774e4de89993e1a0f961c8ef
معادلة التفاعل
levulinic acid
cesium hydroxide
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CESIUM LEVULINATE
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
درجة الحرارة
65°CELSIUS
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىto obtain complete solution
- 2ترشيحThe solution is filtered through No
- 3ترشيح40 filter paper
- 4أخرىto remove dust, etc. The solution
- 5أخرىis then evaporated on a hot plate to 200 g
- 6أخرى, which gives
- 7تركيزa 2 molar concentration, and it
الإجراء التجريبي
46.9 gr. of 99% pure levulinic acid is sluurried in 100 cc. distilled water. 97.3 g. of a 4.22 molar, pure cesium hydroxide solution is added and the temperature is raised to 65° C. to obtain complete solution. The solution is filtered through No. 40 filter paper to remove dust, etc. The solution is then evaporated on a hot plate to 200 g., which gives a 2 molar concentration, and it is then bottled.