تفاعل #451850

معادلة التفاعل

1-Allyloxy-3-phenyl-7-nitro-naphthalene

decaline

→

2-Allyl-3-phenyl-7-nitro-1-naphthol

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةmaintained under nitrogen
2. 2
   درجة الحرارةAfter cooling
3. 3
   أخرىthe crystals formed
4. 4
   غسيلwere washed with petroleum ether
5. 5
   ترشيحfiltered off
6. 6
   أخرىdried at 80° C. under reduced pressure

الإجراء التجريبي

31 g of 1-Allyloxy-3-phenyl-7-nitro-naphthalene prepared in step (3) were gradually heated to 180° C. in 390 ml of decaline, the solution being stirred and maintained under nitrogen. The temperature of 180° C. was maintained for about 1 hour. After cooling, the crystals formed were washed with petroleum ether, filtered off and dried at 80° C. under reduced pressure.

المصدر