تفاعل #44956
ord-60044640ac4f49cfa96a7c565ef0c340
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1ترشيحThe solution was filtered
- 2أخرىthe methanol was evaporated from the filtrate at reduced pressure
- 3أخرىto give a final volume of 30 ml
- 4أخرىdried
الإجراء التجريبي
Pseudomonic acid (10.01 g, 20 mmole) was dissolved in a mixture of methanol/water (50 ml and 36 ml). Calcium oxide (0.78 g, 14 mmole) was added portionwise to the mixture and was stirred for 1 h. The solution was filtered, and the methanol was evaporated from the filtrate at reduced pressure to give a final volume of 30 ml. Water (20 ml) was added to the solution. Then the solution was freeze dried to obtain 9.11 grams of product.