تفاعل #446386

ord-c09605868a7542b1b7a8b6e0550f1f37

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

The general procedure of Example 34 was followed using 1-(2-methoxymethoxyphenyl)-1-(4-methyl-2-methoxyphenyl)ethene and, initially, 3.3 moles of phenylthiomethyl lithium reagent per mole of olefin. The title compound was obtained as a clear oil in 44 percent yield and its structure was verified by proton NMR spectroscopy.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04999448uspto-grants-1991_03