تفاعل #445377

ord-31e0f680e83a4e5bbd90c0566663e97b

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

Methyl 5-fluoro-2-nitrobenzoate was reacted with the sodium salt of 4-chloro-3-methylphenol (prepared from sodium hydride and the phenol) in dimethylformamide at 100° C. for 2.5 hours and the resulting methyl 5(4-chloro-3-methylphenoxy)-2-nitrobenzoate isolated in the usual way; the ester had a melting point of 85°-87° C.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US04465508uspto-grants-1984_08