تفاعل #440595

ord-65e4863b74a84f75b8f25ed37ec71346

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThis mixture stood still for reaction at 200 degrees centigrade for thirty hours
  2. 2
    استخلاصwas extracted by chloroform

الإجراء التجريبي

Then, two equivalents of di-p-tolylamine, potassium carbonate, and copper power were added to the thus obtained dibromobenzo[a]perylene. This mixture stood still for reaction at 200 degrees centigrade for thirty hours. After reactant solution was diluted with water, reactant was extracted by chloroform. Thereafter, the reactant was refined in a conventional manner to thereby obtain bis(di-p-tolylamino)benzo[a]perylene.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US06753097B2uspto-grants-2004_06