تفاعل #440594

ord-578cd3aeae8f4393bac7827830475f3f

المذيبات

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

المعالجة

  1. 1
    أخرىThis mixture stood still for reaction at 200 degrees centigrade for thirty hours
  2. 2
    استخلاصwas extracted by chloroform

الإجراء التجريبي

Then, di-p-tolylamine, potassium carbonate, and copper power were added to the thus obtained bromobenzo[a]perylene. This mixture stood still for reaction at 200 degrees centigrade for thirty hours. After reactant solution was diluted with water, reactant was extracted by chloroform. Thereafter, the reactant was refined in a conventional manner to thereby obtain di-p-tolylaminobenzo[a]perylene.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US06753097B2uspto-grants-2004_06