تفاعل #42011

معادلة التفاعل

ethyl oleate

pentanol

→

pentyl oleate

المردود 91.0%

المذيبات

ether

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةwas refluxed
2. 2
   workup.ADDITIONwas added
3. 3
   ترشيحthe catalyst was filtered off
4. 4
   تركيزconcentrated

الإجراء التجريبي

A mixture containing Catalyst A or B (0.05 g) and ethyl oleate (1.55 g, 5 mmol) and pentanol (10 ml) was refluxed with stirring for 40 h. On cooling ether (30 ml) was added and the catalyst was filtered off. The organic washings were combined and concentrated to give pentyl oleate as an oil (1.6 g, 91% yield).

المصدر