تفاعل #41841
ord-38722a7553584aeca29efcd3a8985b6f
معادلة التفاعل
1-hydrazinophthalazine HCL
2-butanone
→
ethanol heptane
المردود 78.0%
المتفاعلات
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىAfter evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone
الإجراء التجريبي
A 10 parts 1-hydrazinophthalazine HCL (0.05 Molar) in 50% methanol-water are mixed with 1 part 2-butanone. After evaporation of solvents, 1-hydrazinophthalazine 2-butanone hydrazone is crystallized from ethanol-heptane (78% yield). [The Journal of Pharmacology and Experimental Therapeutics 205 (2): 418-425 (1978)].