تفاعل #417924

معادلة التفاعل

sodium hydroxide

29

methyl 2-(undec-4Z-enyloxy)benzoate

→

yellow oil

المردود 99.5%

2-(undec-4Z-enyloxy)benzoic acid

المردود 99.5%

المذيبات

methanol

ظروف التفاعل

المعالجة

1. 1
   درجة الحرارةThe solution is refluxed for 24 hours
2. 2
   أخرىAfter evaporating off the solvent
3. 3
   استخلاصextracted with DCM

الإجراء التجريبي

500 μL of 1 N sodium hydroxide solution (500 μmol) are added portionwise to 80 mg of 29 (263 μmol) in methanol (3 mL). The solution is refluxed for 24 hours. After evaporating off the solvent, the reaction medium is acidified with 0.5 N HCl and extracted with DCM. 76 mg of a yellow oil are obtained, i.e. a yield of 99%.

المصدر