تفاعل #414891

معادلة التفاعل

4-hydroxybenzophenone

chlorosulfonyl isocyanate

→

title compound

المردود 58.4%

Sulfamic acid 4-benzoylphenyl ester

المردود 58.4%

المذيبات

toluene

ظروف التفاعل

المعالجة

1. 1
   أخرىThis compound was prepared

الإجراء التجريبي

This compound was prepared according to the procedure used in Example 84. A mixture of 9.9 g (0.05 mole) of 4-hydroxybenzophenone, 7.1 g (0.0505 mole) of chlorosulfonyl isocyanate and 75 ml of toluene gave 8.1 g (58%) of the title compound as off-white flakes, mp 131°-133° C.

المصدر