تفاعل #414464

معادلة التفاعل

1,3-dimethyl-3-(2-ethylhexanoylperoxy)butyl chloroformate

hydrazine

phosgene

1,3-Dimethyl-3-(2-ethylhexanoylperoxy)butyl chloroformate

→

1,3-Dimethyl-3-(2-ethylhexanoylperoxy)butyl carbazate

ظروف التفاعل

المعالجة

1. 1
   أخرىfollowed by removal of excess phosgene

الإجراء التجريبي

1,3-Dimethyl-3-(2-ethylhexanoylperoxy)butyl carbazate was prepared by reacting 1,3-dimethyl-3-(2-ethylhexanoylperoxy)butyl chloroformate with 11 molar excess of 54% aqueous hydrazine. 1,3-Dimethyl-3-(2-ethylhexanoylperoxy)butyl chloroformate was initially prepared with a purity of 72% by reacting 3-hydroxy-1,1-dimethylbutyl peroxy-2-ethylhexanoate with excess phosgene followed by removal of excess phosgene.

المصدر