تفاعل #414463

ord-182260367f794716ac2a2ea1f6252c70

معادلة التفاعل

CC(CC(C)(C)OOC(C)(C)C)OC(=O)Cl
1,3-dimethyl-3-(t-butylperoxy)butyl chloroformate
NN
hydrazine
→
CC(CC(C)(C)OOC(C)(C)C)OC(=O)NN
1,3-Dimethyl-3-(t-butylperoxy)butyl carbazate

المتفاعلات

CC(CC(C)(C)OOC(C)(C)C)OC(=O)Cl
1,3-dimethyl-3-(t-butylperoxy)butyl chloroformate
NN
hydrazine

الكواشف

لا شيء

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

1,3-Dimethyl-3-(t-butylperoxy)butyl carbazate was prepared by reacting 1,3-dimethyl-3-(t-butylperoxy)butyl chloroformate with 11 molar excess of 54% aqueous hydrazine.

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US05272219uspto-grants-1993_12