تفاعل #41306
ord-99f35be9b4874ec3accc08ee17beeb82
معادلة التفاعل
(S)-tert-butyl 1-(methoxy(methyl)amino)-1-oxopropan-2-ylcarbamate
(3-ethylphenyl)magnesium bromide
THF
→
subtitle compound
(S)-tert-butyl 1-(3-ethylphenyl)-1-oxopropan-2-ylcarbamate
المتفاعلات
الكواشف
لا شيء
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
الإجراء التجريبي
The subtitle compound was prepared analogous to the method described in Example 19 (step 19d). Starting from (S)-tert-butyl 1-(methoxy(methyl)amino)-1-oxopropan-2-ylcarbamate (0.7 g, 3.01 mmol) and freshly made (3-ethylphenyl)magnesium bromide 0.9M solution in THF (5 mL, 4.50 mmol). Yield 817 mg (97%)