تفاعل #3833
ord-ce2fac42f05a4292a71802d2a5aa59d9
معادلة التفاعل
2,2'-dithiobisbenzoyl chloride
pyrrolidine
triethylamine
→
title compound
المردود 60.6%
{2-[2-(pyrrolidine-1-carbonyl)-phenydisulfanyl]-phenyl}-pyrrolidin-1-yl-methanone
المردود 60.6%
الكواشف
لا شيء
المذيبات
ظروف التفاعل
الظروف التفصيلية
See reaction.notes.procedure_details.
المعالجة
- 1أخرىThis compound was prepared
الإجراء التجريبي
This compound was prepared according to the general method of Example 112 using 2,2'-dithiobisbenzoyl chloride (1.0 g, 3.0 mmol) in 15 mL of dichloromethane and pyrrolidine (0.63 mL, 7.5 mmol) and triethylamine (1.2 mL, 9 mmol) in 20 mL of dichloromethane, to give 0.75 g of the title compound as a foam, mp 62°-63° C.;