تفاعل #366620

معادلة التفاعل

15-crown-5

phenylchloroformate

sodium fluoride

→

Phenylfluoroformate

المذيبات

acetonitrile

ظروف التفاعل

المعالجة

1. 1
   أخرىReaction completion

الإجراء التجريبي

To a solution of phenylchloroformate in acetonitrile is charged sodium fluoride. To this mixture is charged the 15-crown-5(“15C5”) at ambient temperature. The reaction mixture is then heated to 40° C. for approximately 16 hrs. Reaction completion is monitored by gas chromatography (“G.C.”).

المصدر