تفاعل #357582

ord-053e7a452de841559a5531b987ffc4c3

معادلة التفاعل

BrCCCCOc1ccc2c(-c3ccc(Br)cc3)csc2c1
6-(4-Bromo-butoxy)-3-(4-bromo-phenyl)-benzo[b]thiophene
COCCNCCOC
bis(2-methoxyethyl)amine
COCCN(CCCCOc1ccc2c(-c3ccc(Br)cc3)csc2c1)CCOC
{4-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-butyl}-bis-(2-methoxy-ethyl)-amine

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

According to the method in example 29, 6-(4-Bromo-butoxy)-3-(4-bromo-phenyl)-benzo[b]thiophene and bis(2-methoxyethyl)amine were converted to yield {4-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-butyl}-bis-(2-methoxy-ethyl)-amine as light brown oil, MS: 492 (MH+, 1Br).

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07449483B2uspto-grants-2008_11