تفاعل #357580

ord-30c98524bf0f419985fabd89d589a58e

معادلة التفاعل

BrCCCOc1ccc2c(-c3ccc(Br)cc3)csc2c1
3-(4-Bromo-phenyl)-6-(3-bromo-propoxy)-benzo[b]thiophene
COCCNCCOC
bis(2-methoxyethyl)amine
COCCN(CCCOc1ccc2c(-c3ccc(Br)cc3)csc2c1)CCOC
{3-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-propyl}-bis-(2-methoxy-ethyl)-amine

ظروف التفاعل

الظروف التفصيلية
See reaction.notes.procedure_details.

الإجراء التجريبي

In analogy to example 3.1, 3-(4-Bromo-phenyl)-6-(3-bromo-propoxy)-benzo[b]thiophene and bis(2-methoxyethyl)amine were converted to yield {3-[3-(4-Bromo-phenyl)-benzo[b]thiophen-6-yloxy]-propyl}-bis-(2-methoxy-ethyl)-amine as light brown oil, MS: 478 (MH+, 1Br).

المصدر

DOI: 10.6084/m9.figshare.5104873.v1براءة الاختراع: US07449483B2uspto-grants-2008_11