تفاعل #346452

معادلة التفاعل

1-[3'-(n-dodecyloxy)-2'-(n-heptyloxy)propyl]imidazole oxalate

potassium carbonate

→

1-[3'-(n-dodecyloxy)-2'-(n-heptyloxy)propyl]imidazole

المذيبات

dichloromethane

ظروف التفاعل

المعالجة

1. 1
   workup.DISSOLUTIONis completely dissolved
2. 2
   أخرىThe organic layer is then separated
3. 3
   غسيلwashed twice with water
4. 4
   تجفيفdried over mgnesium sulfate
5. 5
   أخرىevaporated

الإجراء التجريبي

1-[3'-(n-dodecyloxy)-2'-(n-heptyloxy)propyl]imidazole oxalate (2.3 g.) in 100 ml. of dichloromethane is shaken with excess dilute potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over mgnesium sulfate and evaporated to yield 1-[3'-(n-dodecyloxy)-2'-(n-heptyloxy)propyl]imidazole as a gum.

المصدر