تفاعل #332493

معادلة التفاعل

Dibenzylamine

lithium bromide

(S)-epichlorohydrin

→

colorless Oil

المردود 91.4%

(S)-1-chloro-3-(dibenzylamino)propan-2-ol

المردود 91.4%

ظروف التفاعل

المعالجة

1. 1
   ترشيحFiltered
2. 2
   أخرىthe solvent was evaporated

الإجراء التجريبي

Dibenzylamine (39.4 g, 0.20 mol) and lithium bromide (1.7 g, 20 mmol) were added to (S)-epichlorohydrin (185 g, 2 mol). The mixture was stirred at room temperature (25° C.) for 2 hours, Filtered, and the solvent was evaporated to provide 53 g of colorless Oil in 90% yield.

المصدر