تفاعل #330737

معادلة التفاعل

tert-butyl 2-((4-benzylpiperazin-1-yl)methyl)morpholine-4-carboxylate

trifluoroacetic acid

→

2-((4-benzylpiperazin-1-yl)methyl)morpholine

المذيبات

CH2Cl2

ظروف التفاعل

المعالجة

1. 1
   أخرىThe solvent is removed under reduced pressure

الإجراء التجريبي

To a solution of tert-butyl 2-((4-benzylpiperazin-1-yl)methyl)morpholine-4-carboxylate (600 mg) in CH2Cl2 (10 ml) is added trifluoroacetic acid (1.8 ml), and the mixture is stirred over night. The solvent is removed under reduced pressure to give 2-((4-benzylpiperazin-1-yl)methyl)morpholine*3 TFA (990 mg).

المصدر